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The examination of the Si KL2,3L2,3 line shapes recorded by XPS have allowed one to state the existence of Si(C4−nNn) items. 1000-1200 °C utilizing TMS-NH3-H2 have been investigated utilizing x-ray photoelectron spectroscopy (XPS), Raman spectrometry, Fourier remodel infrared spectrometry (FT-IR), electron power loss spectroscopy (EELS) and 29Si magic-angle spinning nuclear magnetic resonance spectrometry (MAS-NMR). XPS analyses have shown that the main bonds are Si-C, Si-N, and C-C, and have suggested the existence of C-N bonds.
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